9-Bromophenanthrene 9-溴菲
CAS 573-17-1 MFCD00001174
化学结构图
SMILES: Brc1cc2ccccc2c2ccccc12
化学属性
| Mol. Formula | C14H9Br |
|---|---|
| Mol. Weight | 257 |
| Boiling Point | 180-190 |
| Melting Point | 60-64 |
| Density | 1.422 |
| TSCA | No |
| Flash Point | >;230 °F |
| Appearance | 白色结晶。熔点65-66℃，沸点190℃（0.16kPa，升华），相对密度1.409。溶于乙酸、二硫化碳。 |
| Solubility | chloroform: 50 mg/mL, clear |
别名和识别编码
| Chemical Name | 9-Bromophenanthrene |
|---|---|
| MDL Number | MFCD00001174 |
| PubChem Substance ID | 87563821 |
| Beilstein Registry Number | 1869927 |
| CAS Number | 573-17-1 |
| EC Number | 209-351-6 |
| Reaxys-RN | 1869927 |
| Synonym | 9-Bromophenanthrene,95% {uni_hamburg} 9-Phenanthryl bromide 9-溴苯蒽 9-溴菲 9-phenathrylbromide 9-溴苯蒽烯 9-bromo-phenanthrene 9-Phenathryl bromide 9-Bromophenanthrene 9-Bromphenanthren 9-Bromophenanthrene,97% 9-BROMOPHENANTHRENE 9-Bromophenathrene Phenanthrene, 9-bromo- 9-bromo-phenanthren 9-Bromoanth raceme 96% 9-溴代菲 9-溴菲 9-溴苯蒽烯 |
| Chemical Name Translation | 9-溴菲 |
| InChIKey | RSQXKVWKJVUZDG-UHFFFAOYSA-N |
| LabNetwork Molecule ID | LN00222298 |
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分类
- {SNA} Aryl, Building Blocks, C13 to C37+, Chemical Synthesis, Halogenated Hydrocarbons, Organic Building Blocks
- {SA} Aryl, Building Blocks, C13 to C37+, Chemical Synthesis, Halogenated Hydrocarbons, Organic Building Blocks
- {uni_hamburg} no charge; carbocycle; aromatic; large ring; fused rings; 6ring; 10ring; 14ring; 1fragment
- Aryl, Building Blocks, C13 to C37+, Chemical Synthesis, Halogenated Hydrocarbons, Organic Building Blocks
相关文献及参考
- Beil. 5 ,IV,2303
- FT-IR 1 (1), 1032:D / FT-IR 2 (2), 1771:C / FT-NMR 1 (2), 174:C / IR-Spectra (2), 553:D / IR-Spectra (3), 621:D / NMR-Reference 2 (1), 831:D / RegBook 1 (1), 1225:B / Structure Index 1 , 187:B:5 / Vapor Phase 3 , 962:B
- Short: II/3 Title: Luminescence of Organic Substances Author: Schmillen, A.; Legler, R. Editor: Hellwege, K.-H.; Hellwege, A.M. Source: Landolt-Börnstein, New Series Volume: II/3 Year: 1967 ISBN: 3-540-03895-7 ISBN: 978-3-540-03895-5 Internet Resource: DOI:10.1007/b86158 RefComment: 270 figs., VIII, 416 pages. Hardcover Abstract: For more than 1000 luminescent organic substances the most important data are represented as wave numbers of absorption and emission bands, decay times and quantum efficiencies. Additional tables contain further information for restricted groups of substances (figures on typical spectra, wave numbers of sharp single bands, influence of surrounding molecules, etc.).
- Short: EINECS Title: EINECS (European Inventory of Existing Commercial Chemical Substances) Source: Official Journal of the European Communities Volume: C 146 A (15.06.1990) Page: 1 Year: 1990 Internet Resource: http://ecb.jrc.ec.europa.eu/esis/index.php?PGM=ein Publish_Date: 1990/06/15
安全信息
GHS Symbol
- S22 Do not breathe dust 不要吸入粉尘；
- S24/25 Avoid contact with skin and eyes 避免皮肤和眼睛接触；
- S26 In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 眼睛接触后，立即用大量水冲洗并征求医生意见；
- S36/37/39 Wear suitable protective clothing, gloves and eye/face protection 穿戴适当的防护服、手套和眼睛/面保护；
- R36/37/38 Irritating to eyes, respiratory system and skin 对眼睛、呼吸系统和皮肤有刺激性
- P260 Do not breathe dust/fume/gas/mist/vapours/spray. 不要吸入粉尘/烟/气体/烟雾/蒸汽/喷雾。
- P262 Do not get in eyes, on skin, or on clothing. 不要接触眼睛，皮肤或衣服。
TYPE OF TEST : Mutation in microorganisms TEST SYSTEM : Bacteria - Salmonella typhimurium DOSE/DURATION : 50 ug/plate REFERENCE : MUREAV Mutation Research. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1964- Volume(issue)/page/year: 116,91,1983
其他信息
- 用途一:用于有机合成。
- 下游产品:9-腈菲
- TCI Shanghai:9-溴菲 9-Bromophenanthrene,>;98.0%(GC)(573-17-1)
- F:8
- 9-溴菲价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2014/06/02 B0838 9-溴菲 9-Bromophenanthrene 250G 4000元 2014/06/02 B0838 9-溴菲 9-Bromophenanthrene 25G 565元 2010/06/21 107240250 9-溴菲 9-Bromophenanthrene 96% 25 GR 706元
- 图谱信息:9-溴菲(573-17-1)核磁图( 1 HNMR) 9-溴菲(573-17-1)红外图谱(IR1) 9-溴菲(573-17-1)红外图谱(IR2) 9-溴菲(573-17-1)质谱(MS) 9-溴菲(573-17-1)核磁图( 13 CNMR)
- Hazard Note:Irritant
- 上游原料:菲
- Sigma Aldrich:573-17-1(sigmaaldrich)
- 海关编码:29036990
- Alfa Aesar:9-溴菲9-溴苯蒽烯,95% 9-Bromophenanthrene, 98%(573-17-1)
- Acros Organics:9-溴代菲 9-Bromophenanthrene, 96%(573-17-1)
- MOL 文件:573-17-1.mol
- 方法一:将菲溶于干燥的四氯化碳，加热回流，滴加溴素，继续回流逸尽生成的溴化氢。反应液减压蒸除溶剂，继续减压蒸馏，收集177-190℃（0.16kPa）馏分，即为9-溴菲，产率90%-94%。
- MSDS 信息:9-Bromophenanthrene(573-17-1).msds
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