Diethyl hydrazine-1,2-dicarboxylate 肼二羧酸二乙酯

CAS 4114-28-7 MFCD00009101

化学结构图

4114-28-7
SMILES: CCOC(=O)NNC(=O)OCC

化学属性

Mol. FormulaC6H12N2O4
Mol. Weight176.17
Boiling Point250 °C at 760 mmHg
Melting Point131-133 °C
TSCAYes
Appearance 白色晶体。熔点132-134℃，沸点250℃。

别名和识别编码

Chemical NameDiethyl hydrazine-1,2-dicarboxylate
Synonym Diethyl hydrazine-1,2-dicarboxylate {LY} Diethyl hydrazine-1,2-dicarboxylate {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-dicarboxylate {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} Diethyl hydrazine-1,2-d
Beilstein Registry Number1781585
PubChem Substance ID77758
CAS Number4114-28-7
EC Number223-902-8
MDL NumberMFCD00009101
Chemical Name Translation肼二羧酸二乙酯
InChIKeyJXMLAPZRDDWRRV-UHFFFAOYSA-N
LabNetwork Molecule IDLN01795805
InChIInChI=1S/C6H12N2O4/c1-3-11-5(9)7-8-6(10)12-4-2/h3-4H2,1-2H3,(H,7,9)(H,8,10)
Canonical SMILESO=C(NNC(OCC)=O)OCC
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分类

  • Building Blocks, Chemical Synthesis, Hydrazines, Nitrogen Compounds, Organic Building Blocks
  • {SNA} Building Blocks, Chemical Synthesis, Hydrazines, Nitrogen Compounds, Organic Building Blocks

相关文献及参考

  • Beil. 3 ,IV,175
  • FT-IR 1 (1), 776:C / FT-IR 2 (1), 1309:D / FT-NMR 1 (1), 1267:C / IR-Spectra (2), 401:E / IR-Spectra (3), 454:A / NMR-Reference 2 (1), 653:A / RegBook 1 (1), 911:A / Structure Index 1 , 140:D:5
  • In the presence of CuCl/ phenanthroline catalyst, promotes the aerobic oxidation of a number of alcohols to aldehydes or ketones: J. Org. Chem., 64, 2433 (1999). See also Di-tert-butyl­ hydrazodicarboxyl­ate, L00280.

安全信息

WGK Germany3
Personal Protective Equipment Eyeshields, Gloves, type N95 (US), type P1 (EN143) respirator filter
Safety Statements
  • S22 Do not breathe dust 不要吸入粉尘；
  • S24/25 Avoid contact with skin and eyes 避免皮肤和眼睛接触；
Storage condition 2-8°C {LY} 2-8°C {} {LY} 2-8°C {} {} {LY} 2-8°C {} {} {} {LY} 2-8°C {} {} {} {} {LY} 2-8°C {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {LY} 2-8°C {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} { {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {} {

其他信息

  • 下游产品:偶氮二甲酸二乙酯
  • 1,2-肼二羧酸二乙酯价格(试剂级):更新日期 产品编号 产品名称 包装 价格 2010/05/25 L01133 肼二羧酸二乙酯, 98+% Diethyl hydrazodicarboxylate, 98+% 25g 468元 2010/05/25 L01133 肼二羧酸二乙酯, 98+% Diethyl hydrazodicarboxylate, 98+% 100g 1456元
  • 方法一:将85%水合肼和95%乙醇的混合物冷却到10℃，搅拌下滴加氯甲酸乙酯和碳酸钠溶液，控制加料速度，使氯甲酸乙酯保持过量，并先于碳酸钠溶液滴加完，加料温度保持在20℃以上。加料后继续搅拌反应0.5h，滤出沉淀，用水充分洗涤后在80℃真空干燥，得成品，产率81-85%。
  • Alfa Aesar:肼二羧酸二乙酯,98+% Diethyl hydrazodicarboxylate, 98+%(4114-28-7)
  • 用途一:有机合成中间体。
  • Sigma Aldrich:4114-28-7(sigmaaldrich)
  • 上游原料:氯甲酸乙酯
  • MOL 文件:4114-28-7.mol

系列性分类

  1. Chemical Synthesis 化学合成
  2. Building Blocks 合成砌块
  3. Organic Building Blocks 有机砌块
  4. Nitrogen Compounds 氮化合物
  5. Hydrazines - Nitrogen Compounds
  1. Chemical Synthesis 化学合成
  2. Building Blocks 合成砌块
  3. Organic Building Blocks 有机砌块
  4. Nitrogen Compounds 氮化合物
  5. Hydrazines - Nitrogen Compounds

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